反应条件
n-butyllithium in tetrahydrofuran
N2 atmosphere; addn. of BuLi to soln. of PhMe and t-BuOK (-75°C), then 5 h at -50°C, addn. to Bu3SnCl soln. (-75°C), warming to 25°C; pouring into H2O, extn. (hexane), washing (H2O, aq. NaCl), evapn., distn. (reduced pressure); elem. anal.;
参考文献
Desponds, Olivier; Schlosser, Manfred
Journal of Organometallic Chemistry, 1991 , vol. 409, # 1-2 p. 93 - 101
