in not given dropwise addn. of thionyl chloride to tetraalkyltin(IV) compd. under dry N2 atmosphere under ice cooling, warming to room temp., refluxing for 30 min; distn. (removal of excess of SOCl2), cooling resulting liquids, sepn., elem. anal.;
参考文献
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical and Analytical, , vol. 22, # 3 p. 246 - 247
in not given dropwise addn. of thionyl chloride to tetraalkyltin(IV) compd. under dry N2 atmosphere under ice cooling, warming to room temp., refluxing for 30 min; distn. (removal of excess of SOCl2), cooling resulting liquids, sepn., elem. anal.;
参考文献
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical and Analytical, , vol. 22, # 3 p. 246 - 247
Manulkin, Z. M.
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 299 - 305
C.A., 1948 , p. 6742
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Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.2.4.8, page 76 - 79
