1: diethoxyphosphoryl-acetic acid ethyl ester With sodium hydride in tetrahydrofuran; mineral oil 0.5 h; Cooling with ice; 2: acetophenone in tetrahydrofuran; mineral oil T=20°C;
参考文献
Yilmaz, E. Vildan Burgaz; Yilmaz, Mehmet; Oektemer, Atilla
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potassium carbonate in tetrahydrofuran; water T=20°C; Horner-Wadsworth-Emmons reaction; pH=11.6; 17 h;
参考文献
Quaedflieg, Peter J. L. M.; Kesteleyn, Bart R. R.; Wigerinck, Piet B. T. P.; Goyvaerts, Nicolaas M. F.; Vijn, Robert Jan; Liebregts, Constantinus S. M.; Kooistra, Jaap H. M. H.; Cusan, Claudia
Organic Letters, 2005 , vol. 7, # 26 p. 5917 - 5920
1: 1,2,5,6-diisopropylidine-D-manitol With sodium periodate; sodium carbonate in water T=0 - 22°C; 1 h; 2: diethoxyphosphoryl-acetic acid ethyl ester With potassium carbonate in water 18 h; Further stages.;
参考文献
Powell, Sharon A.; Tenenbaum, Jason M.; Woerpel
Journal of the American Chemical Society, 2002 , vol. 124, # 43 p. 12648 - 12649
