3-(1H-咪唑-1-基)-哌啶合成路线 （共 2 条）
反应条件
5 Pd(II)/C(eggshell); hydrogen in methanol
T=80°C; P=76005.1 Torr; 24 h;
参考文献
Shevchuk, Nadiia V.; Liubchak, Kostiantyn; Nazarenko, Kostiantyn G.; Yurchenko, Aleksandr A.; Volochnyuk, Dmitriy M.; Grygorenko, Oleksandr O.; Tolmachev, Andrey A.
Synthesis (Germany), 2012 , vol. 44, # 13 art. no. SS-2012-Z0299-OP, p. 2041 - 2048
反应条件
1.1: copper(l) iodide; N-methyl-2-(methylamino)ethylamine / N,N-dimethyl-formamide / 12 h / Reflux; Inert atmosphere
1.3: 0.5 h
2.1: 5 Pd(II)/C(eggshell); hydrogen / methanol / 24 h / 80 °C / 76005.1 Torr
View Scheme
参考文献
Shevchuk, Nadiia V.; Liubchak, Kostiantyn; Nazarenko, Kostiantyn G.; Yurchenko, Aleksandr A.; Volochnyuk, Dmitriy M.; Grygorenko, Oleksandr O.; Tolmachev, Andrey A.
Synthesis (Germany), 2012 , vol. 44, # 13 art. no. SS-2012-Z0299-OP, p. 2041 - 2048
