2-特戊酰氨基-6-甲基吡啶合成路线 (共 7 条)
反应条件
triethylamine in dichloromethane T=20°C; 24 h; Inert atmosphere;
参考文献
Fray, M. Jonathan; Gillmore, Adam T.; Glossop, Melanie S.; McManus, David J.; Moses, Ian B.; Praquin, Celine F.B.; Reeves, Keith A.; Thompson, Lisa R.
Organic Process Research and Development, 2010 , vol. 14, # 1 p. 263 - 271
反应条件
triethylamine in dichloromethane
参考文献
Dalton Transactions, , vol. 42, # 33 p. 12005 - 12014
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane 8 h; RefluxInert atmosphere;
参考文献
Peterson, Ryan L.; Himes, Richard A.; Kotani, Hiroaki; Suenobu, Tomoyoshi; Tian, Li; Siegler, Maxime A.; Solomon, Edward I.; Fukuzumi, Shunichi; Karlin, Kenneth D.
Journal of the American Chemical Society, 2011 , vol. 133, # 6 p. 1702 - 1705
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane 6 h; Heatingirradiation;
参考文献
Goswami, Shyamaprosad; Dey, Swapan; Jana, Subrata
Tetrahedron, 2008 , vol. 64, # 27 p. 6358 - 6363
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane T=80°C; Bromination; 6 h;
参考文献
Harata, Manabu; Hasegawa, Koji; Jitsukawa, Koichiro; Masuda, Hideki; Einaga, Hisahiko
Bulletin of the Chemical Society of Japan, 1998 , vol. 71, # 5 p. 1031 - 1038
反应条件
selenium(IV) oxide in acetic acid
0.416667 h; Heatingmicrowave;
参考文献
Goswami, Shyamaprosad; Adak, Avijit Kumar
Synthetic Communications, 2003 , vol. 33, # 3 p. 475 - 480
反应条件
1: NBS; AIBN / CCl4 / 3.5 h / 80 °C
2: Na2CO3 / acetonitrile / 60 °C
3: HCl; water / 70 °C
View Scheme
参考文献
Rivas, Juan C. Mareque; Salvagni, Emiliano; Rosales, Rafael Torres Martin de; Parsons, Simon
Dalton Transactions, 2003 , # 17 p. 3339 - 3349