3-氯-1,2-二乙酰氧基丙烷合成路线 （共 13 条）
反应条件
porcine pancreatic lipase; sodium methylate 1) H2O (pH:7), r.t., 2) MeOH, r.t., 4h; Multistep reaction;
参考文献
Poppe, Laszlo; Novak, Lajos; Kajtar-Peredy, Maria; Szantay, Csaba
Tetrahedron: Asymmetry, 1993 , vol. 4, # 10 p. 2211 - 2218
反应条件
porcine pancreatic lipase; sodium methylate 1) H2O (pH:7), r.t., 2) MeOH, r.t., 4h; Multistep reaction;
参考文献
Poppe, Laszlo; Novak, Lajos; Kajtar-Peredy, Maria; Szantay, Csaba
Tetrahedron: Asymmetry, 1993 , vol. 4, # 10 p. 2211 - 2218
反应条件
sodium hydroxide
0.0138889 h; microwave irradiation;
参考文献
Rajabi, Fatemeh; Saidi, Mohammad R.
Synthetic Communications, 2005 , vol. 35, # 3 p. 483 - 491
反应条件
tributylphosphine in toluene
Heating;
参考文献
Fan, Ren-Hua; Hou, Xue-Long
Tetrahedron Letters, 2003 , vol. 44, # 23 p. 4411 - 4413
参考文献
Seelig
Chemische Berichte, 1891 , vol. 24, p. 3466
Full Text Show Details
Wegscheider; Zmerzlikar
Monatshefte fuer Chemie, 1913 , vol. 34, p. 1066
反应条件
acetylsalicylic acid chloride
1) 25 deg C, 10 min, 2) 80 deg C, 2 h;
参考文献
Talekar, D. G.; Joshi, P. L.; Ramaiah, P.; Rao, A. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 145 - 151
反应条件
1,3-dichloro-1,1,3,3-tetrabutyldistannoxane
T=50°C; Acetylation; 5 h;
参考文献
Orita, Akihiro; Ito, Toshihide; Yasui, Yutaka; Otera, Junzo
Synlett, 1999 , # 12 p. 1927 - 1929
反应条件
1,3-dichloro-1,1,3,3-tetrabutyldistannoxane
T=40°C; Acetylation; 50 h;
参考文献
Orita, Akihiro; Ito, Toshihide; Yasui, Yutaka; Otera, Junzo
Synlett, 1999 , # 12 p. 1927 - 1929
参考文献
Seelig
Chemische Berichte, 1891 , vol. 24, p. 3466
Full Text Show Details
Wegscheider; Zmerzlikar
Monatshefte fuer Chemie, 1913 , vol. 34, p. 1066
参考文献
Rider
Journal of the American Chemical Society, 1932 , vol. 54, p. 773,775
Full Text Show Details
Sjoeberg
Svensk Kemisk Tidskrift, 1941 , vol. 53, p. 454,455
Full Text Show Details
Smith et al.
Acta Chemica Scandinavica (1947-1973), 1950 , vol. 4, p. 1375
