反应条件
in dichloromethane byproducts: LiAsF6; under N2, 1 equiv. of Li-compd., 1 equiv. of Bi-compd. and 2 equiv. of C6Me6 were stirred in CH2Cl2 for 4 h, 5 °C; soln. was concd., held at -24 °C for 2 d, crystals were sepd., another crop was given after 2 d at this temp., elem. anal.; keeping the mother liq. for 2 weeks, Bi, the Bi4OF2Cl6(2+) and C6Me6H(1+)-cation con tg. compds. were formed.;
参考文献
Decken, Andreas; Nikiforov, Grigori B.; Passmore, Jack
Polyhedron, 2005 , vol. 24, # 18 p. 2994 - 3003
