1-溴-3-甲基-2-丁烯合成路线 (共 689 条)
参考文献
Helvetica Chimica Acta, , vol. 22, p. 1287,1290
参考文献
Helvetica Chimica Acta, , vol. 5, p. 750
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 105, p. 72
Chemische Berichte, , vol. 58, p. 279 Anm. 15
反应条件
dimethylammonium 2,4-dichlorophenoxyacetate in tetrahydrofuran Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ochiai, Hirofumi; Tamaru, Yoshinao; Tsubaki, Kazunori; Yoshida, Zen-ichi
Journal of Organic Chemistry, 1987 , vol. 52, # 19 p. 4418 - 4420
反应条件
potassium carbonate in acetone Heating;
参考文献
Row; Brown; Stachulski; Lennard
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 8 p. 1604 - 1610
参考文献
Spaeth; Vierhapper
Chemische Berichte, 1938 , vol. 71, p. 1667,1671
Monatshefte fuer Chemie, 1939 , vol. 72, p. 179,187
反应条件
phosphoric acid; sulfuric acid in water T=40 - 90°C; Inert atmosphere;
参考文献
Zhou, Shaodong; Liao, Zutai; Yuan, Jixin; Qian, Chao; Chen, Xinzhi
Research on Chemical Intermediates, 2013 , vol. 39, # 9 p. 4121 - 4125
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane T=20°C; 2 h;
参考文献
Organic Process Research and Development, , vol. 9, # 3 p. 278 - 287
反应条件
potassium carbonate in acetone Heating;
参考文献
NEUROGEN CORPORATION; AVENTIS PHARMACEUTICALS INC.
Patent: WO2005/23806 A2, 2005 ;
Location in patent: Page/Page column 59 ;
WO 2005/023806 A2
反应条件
1: 92 percent / K2CO3 / acetone / 1.5 h / Heating 2: Bu3SnH, AIBN / toluene / 20 h / 95 °C View Scheme
参考文献
Bolm, Carsten; Ewald, Martina; Zehnder, Margareta; Neuburger, Markus A.
Chemische Berichte, 1992 , vol. 125, # 2 p. 453 - 458