1-溴-3-甲基-2-丁烯合成路线 （共 689 条）
反应条件
sodium in diethyl ether
48 h; Heating;
参考文献
Bouzbouz; Kirschleger
Synthesis, 1994 , # 7 p. 714 - 718
反应条件
Yield given. Multistep reaction;
参考文献
Cristau, Henri-Jean; Ribeill, Yves
Synthesis, 1988 , # 11 p. 911 - 912
参考文献
Baldwin,J.E.; Armstrong,C.H.
Journal of the Chemical Society [Section] D: Chemical Communications, 1970 , p. 631 - 632
反应条件
potassium carbonate in tetrahydrofuran
16.16 - 18.16 h;
参考文献
NEUROPHARMA, S.A.
Patent: WO2008/15240 A1, 2008 ;
Location in patent: Page/Page column 45 ;
WO 2008/015240 A1
反应条件
potassium fluoride in acetonitrile
4.5 h; Heating;
参考文献
Pace, Vittorio; Martinez, Fernando; Fernandez, Maria; Sinisterra, Jose V.; Alcantara, Andres R.
Organic Letters, 2007 , vol. 9, # 14 p. 2661 - 2664
反应条件
indium in water; acetonitrile
T=70°C; 1 h;
参考文献
Kyung Ho Kang; Kyung Il Choi; Hun Yeong Koh; Kim; Bong Young Chung; Yong Seo Cho
Synthetic Communications, 2001 , vol. 31, # 15 p. 2277 - 2286
反应条件
1: benzene
2: concentrated methanolic KOH-solution
View Scheme
参考文献
Claisen
Journal fuer Praktische Chemie (Leipzig), 1922 , vol. <2> 105, p. 72
Chemische Berichte, 1925 , vol. 58, p. 279 Anm. 15
反应条件
hexamethyl-distannane in benzene
T=25°C; 5 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yanagisawa, Akira; Noritake, Yoshiyuki; Yamamoto, Hisashi
Chemistry Letters, 1988 , p. 1899 - 1902
反应条件
hexamethyl-distannane in benzene
T=25°C; 5 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yanagisawa, Akira; Noritake, Yoshiyuki; Yamamoto, Hisashi
Chemistry Letters, 1988 , p. 1899 - 1902
反应条件
hexamethyl-distannane in benzene
T=25°C; 5 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yanagisawa, Akira; Noritake, Yoshiyuki; Yamamoto, Hisashi
Chemistry Letters, 1988 , p. 1899 - 1902
