1-溴-3-甲基-2-丁烯合成路线 (共 689 条)
参考文献
Padwa, Albert; Kuethe, Jeffrey T.
Journal of Organic Chemistry, 1998 , vol. 63, # 13 p. 4256 - 4268
反应条件
(i) NaH, (ii) /BRN= 1420778/; Multistep reaction;
参考文献
Clark,R.D. et al.
Synthesis, 1975 , p. 635 - 636
参考文献
Smith et al.
Journal of Organic Chemistry, 1939 , vol. 4, p. 340
反应条件
in tetrahydrofuran
addn. of org. bromide to suspn. of activated (HCl or chlorotrimethylsilane) Zn dust (room temp.);
参考文献
Cui, Hua; Li, Ying; Zhang, Songlin
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 14 p. 2862 - 2869
反应条件
in terms of solvents, catalysts, reagents, and temperature; Product distribution;
参考文献
Cuvigny, Therese; Julia, Marc
Journal of Organometallic Chemistry, 1987 , vol. 331, # 1 p. 121 - 138
反应条件
1: PTC
2: 54 percent / silicagel / benzene / 50 °C / in a
3: H2SO4
View Scheme
参考文献
Lombaert, Stephane De; Ghosez, Leon
Tetrahedron Letters, 1984 , vol. 25, # 32 p. 3475 - 3478
反应条件
(i), (ii) KOH; Multistep reaction;
参考文献
Kraus; Yaouanc; Sturtz
European Journal of Medicinal Chemistry, 1975 , vol. 10, # 5 p. 507 - 513
反应条件
sodium hydride in toluene
1.) 60 deg C, 2.5 h, 2.) 35 deg C, 72 h; Yield given. Yields of byproduct given;
参考文献
Fatope, Majekodunmi O.; Okogun, Joseph I.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 7 p. 1601 - 1604
反应条件
sodium hydride in N,N,N',N',N'',N''-hexamethylphosphoric triamide
1.) 60 deg C, 2.5 h, 2.) 35 deg C, 4 h; other solvent, other time, other temperatures; Product distribution;
参考文献
Fatope, Majekodunmi O.; Okogun, Joseph I.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 7 p. 1601 - 1604
反应条件
potassium carbonate; potassium iodide in N,N-dimethyl-formamide
T=20°C; 2 h;
参考文献
Tyrrell, Elizabeth; Tesfa, Kibur Hunie; Millet, Julien; Muller, Christophe
Synthesis, 2006 , # 18 p. 3099 - 3105