4-(叔丁基二甲基甲硅烷基)氧代-1-丁醇合成路线 （共 27 条）
反应条件
sodium hydride in tetrahydrofuran T=0°C; 1 h;
参考文献
Kang, Eun Joo; Cho, Eun Jin; Ji, Mi Kyung; Lee, Young Eun; Shin, Dong Mok; Choi, Soo Young; Chung, Young Keun; Kim, Jong-Seo; Kim, Hie-Joon; Lee, Sueg-Geun; Lah, Myoung Soo; Lee, Eun
Journal of Organic Chemistry, 2005 , vol. 70, # 16 p. 6321 - 6329
反应条件
titanium(IV) isopropylate; magnesium; magnesium bromide in tetrahydrofuran T=20°C; 12 h;
参考文献
Ohkubo, Mutsumi; Mochizuki, Sayaka; Sano, Takeshi; Kawaguchi, Yuuki; Okamoto, Sentaro
Organic Letters, 2007 , vol. 9, # 5 p. 773 - 776
反应条件
[bis(3-methylimidazole-3-ium) tetraethylene glycol] dimesylate in methanol T=20°C; 1.5 h;
参考文献
Jadhav, Arvind H.; Kim, Hern
Tetrahedron Letters, 2012 , vol. 53, # 39 p. 5338 - 5342
反应条件
Ti-HMS; hydrogen; 5 percent palladium-carbon in methanol P=760 Torr; 3 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 39, # 51 p. 9461 - 9464
反应条件
water; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in tetrahydrofuran; dimethyl sulfoxide T=20°C; 0.75 h;
参考文献
Organic Letters, , vol. 4, # 13 p. 2141 - 2144
反应条件
[Bu4N][Fe(CO)3(NO)]; trimesitylphosphane in ethanol T=40°C; Inert atmosphere;
参考文献
Dieskau, Andre P.; Plietker, Bernd
Organic Letters, 2011 , vol. 13, # 20 p. 5544 - 5547
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane T=20°C; 8.5 h;
参考文献
Sharma; Prasad, T. Rajendra; Srinivas, Rakesh B.
Synthetic Communications, 2004 , vol. 34, # 5 p. 941 - 950
反应条件
1: 4-hydroxybutanol With sodium hydride in tetrahydrofuran T=20°C; 0.75 h; Inert atmosphere; 2: tert-butyldimethylsilyl chloride in tetrahydrofuran T=20°C; 0.75 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 19, # 46 p. 15604 - 15614
反应条件
[t-Bu2SnOH(Cl)]2 in methanol T=30°C; Deacetylation; 4 h;
参考文献
Orita, Akihiro; Hamada, Yuuki; Nakano, Takehiko; Toyoshima, Shinji; Otera, Junzo
Chemistry - A European Journal, 2001 , vol. 7, # 15 p. 3321 - 3327
反应条件
2-hydroxymethyl-phenol in ethanol 10 h; UV-irradiation;
参考文献
Nishikubo, Yuichi; Kanzaki, Shinya; Matsumura, Shuichi; Toshima, Kazunobu
Tetrahedron Letters, 2006 , vol. 47, # 46 p. 8125 - 8128
