in further solvent(s)
byproducts: ZnBr2; Electrolysis; excess of CF2BrCl in N-methyl-2-pyrrolidone (NMP), sacrificial Zn anode,1 V, at room temp.; detd. by (19)F NMR studies;
参考文献
Grobe, Joseph; Hegge, Joachim
Zeitschrift fur Anorganische und Allgemeine Chemie, 2008 , vol. 634, # 11 p. 1975 - 1990
in further solvent(s)
byproducts: ZnBr2; Electrolysis; excess of CF3Br in N-methyl-2-pyrrolidone (NMP), sacrificial Zn anode, 1V, at room temp.; detd. by (19)F NMR studies;
参考文献
Grobe, Joseph; Hegge, Joachim
Zeitschrift fur Anorganische und Allgemeine Chemie, 2008 , vol. 634, # 11 p. 1975 - 1990
1: water; Ba(OH)2 / 5 h / |Reflux
2: potassium hydroxide / water / 2.17 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
ARIZONA BOARD OF REGENTS, A BODY CORPORATE OF THE STATE OF ARIZONA, ACTING FOR AN ON BEHALF OF ARIZONA STATE UNIVERSITY; MADATHIL, Manikandadas, Mathilakathu; KHDOUR, Omar; HECHT, Sidney
Patent: WO2014/59158 A1, 2014 ;
Mitrasov, Yu. N.; Mikhailova, O. N.; Yal'tseva, N. S.; Nikiforov, N. G.; Kormachev, V. V.
J. Gen. Chem. USSR (Engl. Transl.), 1987 , vol. 57, # 6 p. 1417 - 1418,1268
