乙基[(1R)-8-乙基-1,3,4,9-四氢吡喃并[3,4-b]吲哚-1-基]乙酸酯合成路线 (共 3 条)
反应条件
tin(IV) chloride in dichloromethane T=20°C; 2 h;
参考文献
CHEMI SPA
Patent: US2005/14953 A1, 2005 ;
Location in patent: Page column 2 ;
反应条件
tin(IV) chloride in tetrahydrofuran; dichloromethane 4 h; Heating / reflux;
参考文献
Cephalon, Inc.
Patent: US2006/167259 A1, 2006 ;
Location in patent: Page/Page column 10 ;
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
T=20°C; Inert atmosphere;
参考文献
Craighead, Mark; Palin, Ronald; Murray, Neil; Lindsay, Derek
Patent: US2013/225594 A1, 2013 ;
Location in patent: Paragraph 0362; 0363 ;