in benzene-d6
all manipulations under dry Ar atm.; equimolar amt. of B compd. added tosoln. of Si compd. in one portion at room temp., kept for several h at room temp.; monitored by (1)H and (29)Si NMR spectra; distribution of 1,1- and 1,2-allylborated products 25:75;
参考文献
Wrackmeyer, Bernd; Tok, Oleg L.
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2006 , vol. 61, # 3 p. 243 - 251