3,3,5-三甲基环己酮合成路线 (共 69 条)
反应条件
Irradiation; Yield given. Yields of byproduct given;
参考文献
Micheau, J. C.; Paillous, N.; Lattes, A.
Bulletin de la Societe Chimique de France, 1985 , # 2 p. 257 - 263
反应条件
Irradiation; Yield given. Yields of byproduct given;
参考文献
Micheau, J. C.; Paillous, N.; Lattes, A.
Bulletin de la Societe Chimique de France, 1985 , # 2 p. 257 - 263
反应条件
Irradiation; Yields of byproduct given;
参考文献
Micheau, J. C.; Paillous, N.; Lattes, A.
Bulletin de la Societe Chimique de France, 1985 , # 2 p. 257 - 263
反应条件
in isopropyl alcohol
2 h; Heatingalso with other hindered cyclic ketones; Product distribution;
参考文献
Nasipuri, Dhanonjoy; Sarkar, Ashis; Konar, Samir K.; Ghosh, Amitabha
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 3 p. 212 - 215
反应条件
in tetrahydrofuran
T=-78 - 20°C;
参考文献
Lipshutz, Bruce H.; Ghorai, Subir
Organic Letters, 2009 , vol. 11, # 3 p. 705 - 708
参考文献
Marcou,A.; Normant,H.
Bulletin de la Societe Chimique de France, 1965 , p. 3491 - 3494
反应条件
1: Methyltriphenylphosphonium bromide With sodium hydride in dimethyl sulfoxide
T=20°C; 1 h;
2: 3,3,5-trimethyl-cyclohexanone in dimethyl sulfoxide
T=50°C; Wittig reaction; 18 h; Further stages.;
参考文献
Weijers, Carel A. G. M.; Koenst, Paul M.; Franssen, Maurice C. R.; Sudhoelter, Ernst J. R.
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 19 p. 3106 - 3114
反应条件
(i) PhLi, Et2O, (ii) /BRN= 507452/; Multistep reaction;
参考文献
Landor,S.R. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1973 , p. 473 - 478
参考文献
Shell Devel. Co.
Patent: US2442958 , 1944 ;
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Qudrat-i-Khuda; Mukherji
Journal of the Indian Chemical Society, 1946 , vol. 23, p. 435,439
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Birch; Johnson
Journal of the Chemical Society, 1951 , p. 1493,1495