in chloroform
slow addn. of 10 mmol Sb(OC2H5)3 in chloroform with stirring to a boiling CHCl3 soln. of 15 mmol HS(CH2)2SH; boiling for 1 h; pptn. on cooling down;; recrystallization from chloroform;;
参考文献
Hoffmann, Harald M.; Draeger, Martin
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1986 , vol. 41, # 11 p. 1455 - 1460
