1: 89 percent / BuLi / tetrahydrofuran / 1 h / Ambient temperature 2: 16 percent / NaH / tetrahydrofuran / 1.) 0 deg C, 0.5 h, 2.) reflux, 2 h View Scheme
参考文献
Torr, Richard S.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 1169 - 1172
Torr, Richard S.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 1169 - 1172
1: 91 percent / TFA / 1 h / Heating
2: 91 percent / m-chloroperbenzoic acid, sodium carbonate / CH2Cl2 / 72 h / Ambient temperature
View Scheme
参考文献
Torr, Richard S.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 1169 - 1172
1: 87 percent / BuLi / tetrahydrofuran / 1.) -78 deg C, 10 min, 2.) warm to room temperature
2: 91 percent / TFA / 1 h / Heating
3: 91 percent / m-chloroperbenzoic acid, sodium carbonate / CH2Cl2 / 72 h / Ambient temperature
View Scheme
参考文献
Torr, Richard S.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 1169 - 1172
1: 87 percent / BuLi / tetrahydrofuran / 1.) -78 deg C, 10 min, 2.) warm to room temperature
2: 91 percent / TFA / 1 h / Heating
3: 91 percent / m-chloroperbenzoic acid, sodium carbonate / CH2Cl2 / 72 h / Ambient temperature
View Scheme
参考文献
Torr, Richard S.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 1169 - 1172
1: 89 percent / BuLi / tetrahydrofuran / 1 h / Ambient temperature
2: 79 percent / NaH / tetrahydrofuran / 1.) 0 deg C, 0.5 h, 2.) reflux, 2 h
View Scheme
参考文献
Torr, Richard S.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 1169 - 1172
boron trifluoride diethyl etherate in dichloromethane
T=0°C; 6 h;
参考文献
Bell, Andrew; Davidson, Alan H.; Earnshaw, Chris; Norrish, Howard K.; Torr, Richard S.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2879 - 2892
Bell, Andrew; Davidson, Alan H.; Earnshaw, Chris; Norrish, Howard K.; Torr, Richard S.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2879 - 2892
1: 89 percent / BuLi / tetrahydrofuran / 1 h / Ambient temperature
2: 79 percent / NaH / tetrahydrofuran / 1.) 0 deg C, 0.5 h, 2.) reflux, 2 h
3: 72 h / Irradiation
View Scheme
参考文献
Torr, Richard S.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 1169 - 1172
Bell, Andrew; Davidson, Alan H.; Earnshaw, Chris; Norrish, Howard K.; Torr, Richard S.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2879 - 2892
