反应条件
1: 1.) C2H5MgBr, CuCN / 1.) THF, reflux, 30 min, 2.) THF, 25 deg C, 14 h
2: 96 percent / conc. H2SO4 / methanol / 16 h / 25 °C
3: 79 percent / pyridinium chlorochromate / CH2Cl2 / 2 h / 25 °C
View Scheme
参考文献
Elliott, William J.; Needleman, Philip; Sprecher, Howard
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5378 - 5379
