molecular sieve; tris(dimethylamino)-sulphonium difluorotrimethylsilicate in tetrahydrofuran
T=20°C; 1 h; Yield given. Yields of byproduct given;
参考文献
Palomo, Claudio; Aizpurua, Jesus M.; Garcia, Jesus M.; Ganboa, Inaki; Cossio, F. P.; et al.
Journal of Organic Chemistry, 1990 , vol. 55, # 8 p. 2498 - 2503
1: 4-methyl-styrene With dibutylzirconocene in tetrahydrofuran
T=20°C; 1 h;
2: diethyl chlorophosphate in tetrahydrofuran
T=5°C; 6 h;
3: With iodine in tetrahydrofuran
T=20°C; 0.5 h;
Demik, N. N.; Kabachnik, M. M.; Novikova, Z. S.; Beletskaya, I. P.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 1.1 p. 57 - 60
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 1 p. 64 - 68
Demik, N. N.; Kabachnik, M. M.; Novikova, Z. S.; Beletskaya, I. P.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 1.1 p. 57 - 60
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 1 p. 64 - 68
