in tetrahydrofuran addn. of C5H5TiCl3 to a soln. of C5(CH3)4HLi in THF at -20°C, standing for 30 min at room temp.; evapn., washing with hexane, cryst. powder of 70percent (C5(CH3)4H)(C5H5)TiCl2 and 30percent (C5H5)2TiCl2;
参考文献
Courtot, P.; Pichon, R.; Salaun, J. Y.; Toupet, L.
Canadian Journal of Chemistry, 1991 , vol. 69, # 4 p. 661 - 672