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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
87802-71-9
合成路线
（共 60 条）
108-94-1
环己酮
+
87802-71-9
→
反应条件
79801-99-3
+
105273-48-1
反应条件
tetrakis(triphenylphosphine) palladium(0); samarium diiodide in tetrahydrofuran T=20°C; 15 h;
参考文献
Liu, Wei; Zhang, Liang; Yang, Weikang; Zhao, Xiaoming
RSC Advances, 2013 , vol. 3, # 43 p. 19917 - 19919
110-91-8
吗啉
+
87802-71-9
→
反应条件
85620-82-2
+
92040-02-3
反应条件
bis(η3-allyl-μ-chloropalladium(II)) in toluene T=20°C; Product distribution; Further Variations:Reagents;
参考文献
Takeuchi; Ue; Tanabe; Yamashita; Shiga
Journal of the American Chemical Society, 2001 , vol. 123, # 39 p. 9525 - 9534
37746-78-4
4-溴巴豆酸乙酯
+
87802-71-9
→
反应条件
420811-77-4
反应条件
1: methyl (2E)-3-phenyl-2-propenyl carbonate With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; tris-(o-tolyl)phosphine in tetrahydrofuran T=20°C; 0.25 h; 2: 4-Bromo-crotonoic acid ethyl ester With indium in tetrahydrofuran T=65°C; 24 h;
参考文献
Lee, Phil Ho; Sung, Sun-young; Lee, Kooyeon; Chang, Sukbok
Synlett, 2002 , # 1 p. 146 - 148
1833-53-0
2-(三甲基硅氧基)丙烯
+
87802-71-9
→
反应条件
33599-88-1
反应条件
[Rh(1,5-cyclooctadiene)(PMePh2)2]OTf in dichloromethane T=80°C; Substitution; 19 h; Title compound not separated from byproducts;
参考文献
Muraoka; Matsuda; Itoh
Tetrahedron Letters, 2000 , vol. 41, # 45 p. 8807 - 8811
87802-71-9
+
105-53-3
丙二酸二乙酯
→
反应条件
反应条件
1-methyl-piperidine; [Ru(η4-C8H12)(η6-C8H10)] T=80°C; 10 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Zhang, Shi-Wei; Mitsudo, Take-aki; Kondo, Teruyuki; Watanabe, Yoshihisa
Journal of Organometallic Chemistry, 1993 , vol. 450, # 1.2 p. 197 - 207
75-77-4
三甲基氯硅烷
+
87802-71-9
→
反应条件
40595-34-4
反应条件
tetraethylammonium p-toluenesulfonate in N,N-dimethyl-formamide Ambient temperatureelectrochemical reduction (H-type cell with Pt electrodes);
参考文献
Yoshida, Jun-Ichi; Muraki, Katsuhiko; Funanashi, Hirokatsu; Kawabata, Nariyoshi
Journal of Organometallic Chemistry, 1985 , vol. 284, p. C33 - C35
87802-71-9
+
67-64-1
丙酮
→
反应条件
40596-05-2
反应条件
di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; samarium diiodide in tetrahydrofuran T=25°C; 6 h; Inert atmosphere; regioselective reaction;
参考文献
Liu, Wei; Zhang, Liang; Yang, Weikang; Zhao, Xiaoming
RSC Advances, 2013 , vol. 3, # 43 p. 19917 - 19919
87802-71-9
+
100-46-9
苄胺
→
反应条件
40032-55-1
苄基-((E)-3-苯基-烯丙基)-胺
+
104937-80-6
反应条件
1: With propylamine; O,O'-(R)-(1,1'-dinaphthyl-2,2'-diyl)-N-cyclododecyl-N'-(R,R)-phenylethylphosphoramidite; [Ir(μ-Cl)(1,5-cyclooctadiene)]2 in tetrahydrofuran T=50°C; 0.333333 h; 2: methyl (2E)-3-phenyl-2-propenyl carbonate; benzylamine in tetrahydrofuran T=20°C; 3 h; Product distribution / selectivity;
参考文献
YALE UNIVERSITY
Patent: WO2005/111050 A2, 2005 ;
Location in patent: Page/Page column 53; 55-57 ;
87802-71-9
+
100-46-9
苄胺
→
反应条件
40032-55-1
苄基-((E)-3-苯基-烯丙基)-胺
+
104937-80-6
反应条件
di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; C12H8O2PN(CH(CH3)C6H5)2 in tetrahydrofuran T=25°C; 48 h;
参考文献
YALE UNIVERSITY
Patent: WO2004/24684 A2, 2004 ;
Location in patent: Page 14; 16-17 ;
87802-71-9
+
100-46-9
苄胺
→
反应条件
40032-55-1
苄基-((E)-3-苯基-烯丙基)-胺
反应条件
di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; (S)-(1,1'-binaphthalene-2,2'-dioxy)P(N(R)-CH(o-Tol)Me)2 in tetrahydrofuran T=20°C; 16 h; Product distribution; Further Variations:Reagents;
参考文献
Ohmura, Toshimichi; Hartwig, John F.
Journal of the American Chemical Society, 2002 , vol. 124, # 51 p. 15164 - 15165
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