pyridine; thionyl chloride in toluene
1 h; Heating;
参考文献
Allen, Barbara M.; Hegarty, Anthony F.; O'Neill, Pat; Nguyen, Minh Tho
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1992 , # 6 p. 927 - 934
1: 64 percent / H2SO4, AcOH / 48 h / Ambient temperature
2: 69.2 percent / SOCl2, pyridine / toluene / 1 h / Heating
View Scheme
参考文献
Allen, Barbara M.; Hegarty, Anthony F.; O'Neill, Pat; Nguyen, Minh Tho
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1992 , # 6 p. 927 - 934
1: 91 percent / SeO2 / dioxane; H2O / 7 h / Heating
2: H2O / 0.75 h / Heating
3: 64 percent / aq. KOH / 1 h / 100 °C
4: 64 percent / H2SO4, AcOH / 48 h / Ambient temperature
5: 69.2 percent / SOCl2, pyridine / toluene / 1 h / Heating
View Scheme
参考文献
Allen, Barbara M.; Hegarty, Anthony F.; O'Neill, Pat; Nguyen, Minh Tho
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1992 , # 6 p. 927 - 934
1: 64 percent / aq. KOH / 1 h / 100 °C
2: 64 percent / H2SO4, AcOH / 48 h / Ambient temperature
3: 69.2 percent / SOCl2, pyridine / toluene / 1 h / Heating
View Scheme
参考文献
Allen, Barbara M.; Hegarty, Anthony F.; O'Neill, Pat; Nguyen, Minh Tho
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1992 , # 6 p. 927 - 934
