5-甲基-3-苯基-4-异噁唑甲醛合成路线 （共 12 条）
反应条件
manganese(IV) oxide in dichloromethane T=20°C; Inert atmosphere;
参考文献
Kalin, Jay H.; Zhang, Hankun; Gaudrel-Grosay, Sophie; Vistoli, Giulio; Kozikowski, Alan P.
ChemMedChem, 2012 , vol. 7, # 3 p. 425 - 439
反应条件
1: lithium aluminum hydride / tetrahydrofuran / 1.) 0 deg C, 2.) room temperature 2: 59 percent / potassium dichromate, Adogen-464 / ethyl acetate View Scheme
参考文献
Synthetic Communications, , vol. 13, # 10 p. 817 - 822
反应条件
1.1: NaOMe / methanol 1.2: methanol / 4 h / 0 °C 2.1: 100 percent / LiAlH4 / diethyl ether / 1 h / 40 °C 3.1: PCC / CH2Cl2 / 0.5 h / 20 °C View Scheme
参考文献
Synthesis, , # 9 p. 1347 - 1356
反应条件
1: 100 percent / LiAlH4 / diethyl ether / 1 h / 40 °C 2: PCC / CH2Cl2 / 0.5 h / 20 °C View Scheme
参考文献
Synthesis, , # 9 p. 1347 - 1356
反应条件
1: N-chloro-succinimide; aluminum oxide / 40 °C / Microwave irradiation 2: triethylamine / tetrahydrofuran / 1 h / 70 °C / Microwave irradiation 3: water; sodium hydroxide / methanol / 4 h / 60 °C 4: borane-THF / tetrahydrofuran / 0 - 20 °C 5: manganese(IV) oxide / dichloromethane / 20 °C / Inert atmosphere View Scheme
参考文献
ChemMedChem, , vol. 7, # 3 p. 425 - 439
反应条件
1: water; sodium hydroxide / methanol / 4 h / 60 °C 2: borane-THF / tetrahydrofuran / 0 - 20 °C 3: manganese(IV) oxide / dichloromethane / 20 °C / Inert atmosphere View Scheme
参考文献
ChemMedChem, , vol. 7, # 3 p. 425 - 439
反应条件
in diethyl ether T=0 - 5°C; Cycloaddition; 48 h; Product distribution; Further Variations:Reaction partners;
参考文献
Tetrahedron, , vol. 56, # 25 p. 4299 - 4309
反应条件
1: toluene; PCl5 2: SnCl2; HCl View Scheme
参考文献
Gazzetta Chimica Italiana, , vol. 68, p. 411,416
反应条件
hydrogenchloride; tin(ll) chloride
参考文献
Gazzetta Chimica Italiana, , vol. 68, p. 411,416
反应条件
potassium permanganate
参考文献
Quilico; Panizzi
Gazzetta Chimica Italiana, 1938 , vol. 68, p. 411,416
