2,4,6-三甲基苯胺合成路线 (共 254 条)
反应条件
acetic acid in water 264 h;
参考文献
Goldstein, Stephen L.; McNelis, Edward
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1613 - 1620
反应条件
ammonium acetate; potassium hexacyanoferrate(III) in tetrahydrofuran; water T=45°C; 240 h; other reaction condition, other amines; MechanismProduct distribution;
参考文献
Goldstein, Stephen L.; McNelis, Edward
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1613 - 1620
反应条件
water; chromium oxychloride 1.) CCl4, 0-5 deg. C, 80 min.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Nallaiah, C.; Strickson, J. A.
Tetrahedron, 1986 , vol. 42, # 14 p. 4083 - 4088
反应条件
water; chromium oxychloride; 1-amino-2,4,6-trichlorobenzene 1.) CCl4, 0-5 deg. C, 80 min.; Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Nallaiah, C.; Strickson, J. A.
Tetrahedron, 1986 , vol. 42, # 14 p. 4083 - 4088
反应条件
water; chromium oxychloride 1.) CCl4, 0-5 deg. C, 80 min.; Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Nallaiah, C.; Strickson, J. A.
Tetrahedron, 1986 , vol. 42, # 14 p. 4083 - 4088
参考文献
Chapman; Saunders
Journal of the Chemical Society, 1941 , p. 496,499
反应条件
in Gegenwart von Peroxidase-Praeparaten;
参考文献
Chapman; Saunders
Journal of the Chemical Society, 1941 , p. 496,499
反应条件
in ethanol 24 h; Ambient temperature;
参考文献
Vanelle; Maldonado; Jentzer; Crozet; Savornin; Delmas; Gasquet; Timon-David
European Journal of Medicinal Chemistry, 1990 , vol. 25, # 4 p. 321 - 325
反应条件
potassium carbonate in acetonitrile
参考文献
Paczal, Attila; Benyei, Attila C.; Kotschy, Andras
Journal of Organic Chemistry, 2006 , vol. 71, # 16 p. 5969 - 5979
反应条件
toluene-4-sulfonic acid in benzene
参考文献
Neurogen Corporation
Patent: US6355651 B1, 2002 ;
Location in patent: Page column 17 ;
US 6355651 B1