2,4,6-三甲基苯胺合成路线 （共 254 条）
反应条件
in toluene
23 h; Reflux;
参考文献
Saelinger, Daniel; Brueckner, Reinhard
Synlett, 2009 , # 1 p. 109 - 111
反应条件
1: 95 percent / K2CO3 / acetonitrile
2: 92 percent / NaN3 / methanol / Heating
3: 78 percent / LiAlH4 / tetrahydrofuran / Heating
View Scheme
参考文献
Paczal, Attila; Benyei, Attila C.; Kotschy, Andras
Journal of Organic Chemistry, 2006 , vol. 71, # 16 p. 5969 - 5979
反应条件
bis(trimethylaluminum)-1,4-diazabicyclo[2.2.2]octane in tetrahydrofuran
T=130°C; 0.133333 h; Inert atmosphereMicrowave irradiation;
参考文献
Dubois, Nathalie; Glynn, Daniel; McInally, Thomas; Rhodes, Barrie; Woodward, Simon; Irvine, Derek J.; Dodds, Chris
Tetrahedron, 2013 , vol. 69, # 46 p. 9890 - 9897
参考文献
Grammaticakis
Bulletin de la Societe Chimique de France, 1949 , p. 134,144
反应条件
indium tribromide
T=30 - 35°C; 0.5 h;
参考文献
Chankeshwara, Sunay V.; Chakraborti, Asit K.
Synthesis, 2006 , # 16 p. 2784 - 2788
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile
T=82°C; 60 h;
参考文献
Knoelker, Hans-Joachim; Braxmeier, Tobias
Tetrahedron Letters, 1996 , vol. 37, # 33 p. 5861 - 5864
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile
T=82°C; 15 h;
参考文献
Knoelker, Hans-Joachim; Braxmeier, Tobias
Tetrahedron Letters, 1996 , vol. 37, # 33 p. 5861 - 5864
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile
T=82°C; 60 h;
参考文献
Knoelker, Hans-Joachim; Braxmeier, Tobias
Tetrahedron Letters, 1996 , vol. 37, # 33 p. 5861 - 5864
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile
T=82°C; 15 h;
参考文献
Knoelker, Hans-Joachim; Braxmeier, Tobias
Tetrahedron Letters, 1996 , vol. 37, # 33 p. 5861 - 5864
反应条件
in tetrachloromethane
T=20°C; Condensation; Product distribution; Further Variations:SolventsTemperatures;
参考文献
Basel, Yochai; Hassner, Alfred
Journal of Organic Chemistry, 2000 , vol. 65, # 20 p. 6368 - 6380
