N,N-二乙基氯甲酰胺合成路线 （共 193 条）
反应条件
sodium hydride in tetrahydrofuran T=20°C;
参考文献
Hartung, Christian G.; Fecher, Anja; Chapell, Brian; Snieckus, Victor
Organic Letters, 2003 , vol. 5, # 11 p. 1899 - 1902
反应条件
sodium hydride in tetrahydrofuran 3 h; Heating;
参考文献
Nguyen, Tam; Wicki, Markus A.; Snieckus, Victor
Journal of Organic Chemistry, 2004 , vol. 69, # 23 p. 7816 - 7821
反应条件
triethylamine in tetrahydrofuran
参考文献
The Boots Company Limited
Patent: US3952001 A1, 1976 ;
反应条件
triethylamine in tetrahydrofuran
参考文献
The Boots Company Limited
Patent: US3952001 A1, 1976 ;
反应条件
triethylamine in 1,4-dioxane
参考文献
Stanford Research Institute
Patent: US4056535 A1, 1977 ;
反应条件
1: 1.) KH / 1.) THF, r.t., 20 min, 2.) 2 h
2: 86 percent / LDA / tetrahydrofuran / 6 h / -78 °C
View Scheme
参考文献
Zhang, Pingsheng; Gawley, Robert E.
Journal of Organic Chemistry, 1993 , vol. 58, # 12 p. 3223 - 3224
反应条件
Yield given. Multistep reaction;
参考文献
Hiiro, Tomoki; Mogami, Toshiaki; Kambe, Nobuaki; Fujiwara, Shin-Ichi; Sonoda, Noboru
Synthetic Communications, 1990 , vol. 20, # 5 p. 703 - 711
参考文献
Tilles
Journal of the American Chemical Society, 1959 , vol. 81, p. 714,716
反应条件
in dichloromethane
T=0°C; 0.5 h;
参考文献
Kantlehner, Willi; Kapassakalidis, Johannis J.; Speh, Peter; Braeuner, Hans-Juergen
Liebigs Annalen der Chemie, 1980 , # 3 p. 389 - 393
反应条件
1: 1.) t-BuLi/TMEDA / 1.) THF, -78 deg C
2: 1.) TBAF 2.) Et3BHLi / 1.) THF, RT 2.) THF, reflux
View Scheme
参考文献
Cuevas, J.-C.; Patil, P.; Snieckus, V.
Tetrahedron Letters, 1989 , vol. 30, # 43 p. 5841 - 5844
