N,N-二乙基氯甲酰胺合成路线 (共 193 条)
反应条件
triethylamine in dichloromethane
T=0 - 20°C;
参考文献
El-Faham, Ayman; Khattab, Sherine N.; Abdul-Ghani, Mohamed; Albericio, Fernando
European Journal of Organic Chemistry, 2006 , # 6 p. 1563 - 1573
反应条件
in dichloromethane
T=0 - 20°C;
参考文献
Khattab, Sherine Nabil; Hassan, Seham Yassin; Hamed, Ezzat Awad; Albericio, Fernando; Ayman, El-Faham
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 1 p. 75 - 81
反应条件
in benzene
2 h; Ambient temperature;
参考文献
Bestmann, Hans Juergen; Kisielowski, Lothar
Chemische Berichte, 1983 , vol. 116, # 4 p. 1320 - 1326
反应条件
ammonium hydroxide; dimethyl sulfoxide in ethanol
参考文献
Sterling Drug Inc.
Patent: US4008235 A1, 1977 ;
反应条件
1: 2,3-dihydroindole With n-butyllithium in diethyl ether; hexane
T=0 - 20°C; 1 h; Inert atmosphereSchlenk technique;
2: N,N-diethyl carbamoyl chloride in diethyl ether; hexane
T=0 - 20°C; 14 h; Inert atmosphereSchlenk technique;
参考文献
Jiao, Lin-Yu; Oestreich, Martin
Organic Letters, 2013 , vol. 15, # 20 p. 5374 - 5377
参考文献
Sanofi
Patent: US5594023 A1, 1997 ;
反应条件
1: β-naphthol With sodium hydride in ethylene glycol dimethyl ether; mineral oil
T=0 - 23°C; 0.166667 h;
2: N,N-diethyl carbamoyl chloride in ethylene glycol dimethyl ether; mineral oil
T=23°C; 11 h;
参考文献
Quasdorf, Kyle W.; Riener, Michelle; Petrova, Krastina V.; Garg, Neil K.
Journal of the American Chemical Society, 2009 , vol. 131, # 49 p. 17748 - 17749
反应条件
in 1,4-dioxane
T=20°C;
参考文献
Perveen, Shahnaz; Fatima, Nasreen; Khan, Khalid Mohammed; Khan, Ajmal; Ali, Muhammad; Choudhary, Muhammad Iqbal
Journal of the Chemical Society of Pakistan, 2010 , vol. 32, # 3 p. 338 - 343
参考文献
Ozaki; Nagoya
Bulletin of the Chemical Society of Japan, 1957 , vol. 30, p. 444,448
参考文献
AB Leo
Patent: DE2629657 , 1977 ;
Chem.Abstr., 1977 , vol. 86, # 189570