N,N-二乙基氯甲酰胺合成路线 （共 193 条）
参考文献
Tilles
Journal of the American Chemical Society, 1959 , vol. 81, p. 714,716
参考文献
Einhorn; Hamburger
Justus Liebigs Annalen der Chemie, 1908 , vol. 361, p. 126
反应条件
potassium hydroxide in dimethyl sulfoxide; toluene T=8°C; 0.25 h;
参考文献
Len, Christophe; Postel, Denis; Ronco, Gino; Villa, Pierre
Phosphorus, Sulfur and Silicon and Related Elements, 1998 , vol. 133, p. 41 - 59
反应条件
diethyl ether; triethylamine
参考文献
Bestian
Justus Liebigs Annalen der Chemie, 1950 , vol. 566, p. 210,231
Full Text Show Details
Farbw. Hoechst
Patent: DE858847 , 1942 ;
参考文献
ICI
Patent: US2398283 , 1943 ;
反应条件
pyridine in chloroform 50 h; Heating;
参考文献
Cherbuliez,E. et al.
Helvetica Chimica Acta, 1961 , vol. 44, p. 1806 - 1809
参考文献
Hazard,R. et al.
Bulletin de la Societe Chimique de France, 1961 , p. 2089 - 2091
反应条件
potassium carbonate in acetonitrile T=85°C; 18 h;
参考文献
Bedford, Robin B.; Webster, Ruth L.; Mitchell, Charlotte J.
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 23 p. 4853 - 4857
反应条件
1: tert.-butyl lithium With CuCN in tetrahydrofuran T=-30°C; 0.5 h; 2: N,N-diethyl carbamoyl chloride in tetrahydrofuran T=-30 - 0°C; 2 h;
参考文献
Lemoucheux, Laurent; Seitz, Thomas; Rouden, Jacques; Lasne, Marie-Claire
Organic Letters, 2004 , vol. 6, # 21 p. 3703 - 3706
反应条件
1: tert.-butyl lithium With CuCN in diethyl ether T=-30°C; 0.5 h; 2: N,N-diethyl carbamoyl chloride in diethyl ether T=-30 - 0°C; 2 h;
参考文献
Lemoucheux, Laurent; Seitz, Thomas; Rouden, Jacques; Lasne, Marie-Claire
Organic Letters, 2004 , vol. 6, # 21 p. 3703 - 3706
