N,N-二乙基氯甲酰胺合成路线 （共 193 条）
反应条件
potassium hydroxide in acetone T=25 - 30°C; 24 h;
参考文献
D'Amico, John J.; Schafer, Tann
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 8, p. 301 - 304
反应条件
in acetone 1.) 6 h, reflux, 2.) 18 h, 25-30 deg C;
参考文献
D'Amico, John J.; Schafer, Tann
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 8, p. 301 - 304
反应条件
triethylamine T=20°C; 0.333333 h;
参考文献
DIRECTOR GENERAL, DEFENCE RESEARCH and DEVELOPMENT ORGANISATION; RAO, Ambati Narasimha; GANESAN, Kumaran; VIJAYARAGHAVAN, Rajagopalan
Patent: WO2013/65059 A1, 2013 ;
Location in patent: Page/Page column 14 ;
反应条件
1: methyllithium With CuCN in tetrahydrofuran T=-30°C; 0.5 h; 2: N,N-diethyl carbamoyl chloride in tetrahydrofuran T=-30 - 20°C; 2 h;
参考文献
Lemoucheux, Laurent; Seitz, Thomas; Rouden, Jacques; Lasne, Marie-Claire
Organic Letters, 2004 , vol. 6, # 21 p. 3703 - 3706
反应条件
Yield given. Multistep reaction;
参考文献
Hiiro, Tomoki; Mogami, Toshiaki; Kambe, Nobuaki; Fujiwara, Shin-Ichi; Sonoda, Noboru
Synthetic Communications, 1990 , vol. 20, # 5 p. 703 - 711
参考文献
Farbenfabr. Bayer
Patent: DE875807 , 1951 ;
反应条件
in 1,4-dioxane T=50 - 60°C;
参考文献
Perveen, Shahnaz; Mustafa, Sana; Khan, Khalid Mohammed
Journal of the Chemical Society of Pakistan, 2010 , vol. 32, # 2 p. 229 - 234
反应条件
in 1,4-dioxane T=50 - 60°C;
参考文献
Perveen, Shahnaz; Mustafa, Sana; Khan, Khalid Mohammed
Journal of the Chemical Society of Pakistan, 2010 , vol. 32, # 2 p. 229 - 234
反应条件
in 1,4-dioxane T=50 - 60°C;
参考文献
Perveen, Shahnaz; Mustafa, Sana; Khan, Khalid Mohammed
Journal of the Chemical Society of Pakistan, 2010 , vol. 32, # 2 p. 229 - 234
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran 24 h; Reflux;
参考文献
Rieke, Reuben D.; Kim, Seung-Hoi
Tetrahedron Letters, 2012 , vol. 53, # 27 p. 3478 - 3481
