1: With 2,9-dimethyl-1,10-phenanthroline; p-benozquinone; palladium diacetate in acetonitrile T=100°C; Heck reaction; 0.166667 h; microwave irradiation; 2: With silica gel in ethyl acetate Further stages.;
Rh(acac)(dppb) in tetrahydrofuran 18 h; Inert atmosphere; regioselective reaction;
参考文献
Geier, Michael J.; Vogels, Christopher M.; Decken, Andreas; Westcott, Stephen A.
Journal of Organometallic Chemistry, 2009 , vol. 694, # 19 p. 3154 - 3159
[{(η5-C5Me5)IrCl}2(μ-Cl)2] in benzene-d6 18 h; Inert atmosphere;
参考文献
Geier, Michael J.; Vogels, Christopher M.; Decken, Andreas; Westcott, Stephen A.
Journal of Organometallic Chemistry, 2009 , vol. 694, # 19 p. 3154 - 3159