3,5-二叔丁基-4-羟基苄醇合成路线 (共 55 条)
反应条件
sodium hydroxide; sodium tetrahydroborate in methanol 27 h; Ambient temperature;
参考文献
Goulart, Marilia O. F.; Utley, James H. P.
Journal of Organic Chemistry, 1988 , vol. 53, # 11 p. 2520 - 2525
反应条件
diethylamine 11 h; Reflux;
参考文献
WO2011/5735 A1, ;
Page/Page column 8-9 ;
反应条件
N,N,N-trimethyl-1-phenylmethanaminium tribromide in dichloromethane; water 0.5 h; Ambient temperature;
参考文献
Kajigaeshi, Shoji; Morikawa, Yukihiro; Fujisaki, Shizuo; Kakinami, Takaaki; Nishihira, Keigo
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 3 p. 1060 - 1062
参考文献
Journal of the American Chemical Society, , vol. 77, p. 1783
反应条件
1: unter Stickstoff 2: H2O; acetone View Scheme
参考文献
Journal of the American Chemical Society, , vol. 77, p. 1783
反应条件
perchloric acid; water in acetone 28 h; Heating;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. <1> 38, # 12 p. 2530 - 2535
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 12 p. 2765 - 2770
反应条件
perchloric acid in tetrahydrofuran 48 h; Ambient temperature;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1499 - 1508
反应条件
1: 90 percent / H2O / acetone / 1) 1h, reflux, 2) after addition of water 1h, reflux 2: 49 percent / 72percent HClO4, H2O / acetone / 28 h / Heating View Scheme
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. <1> 38, # 12 p. 2530 - 2535
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 12 p. 2765 - 2770
反应条件
1: 100 percent / acetone / Heating 2: 49 percent / 72percent HClO4, H2O / acetone / 28 h / Heating View Scheme
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. <1> 38, # 12 p. 2530 - 2535
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 12 p. 2765 - 2770
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Journal of Organic Chemistry, , vol. 21, p. 1289,1291
Journal of Organic Chemistry, , vol. 24, p. 1251,1256