反应条件
1: hydroxylamine hydrochloride; sodium sulfate; hydrogenchloride / water / 65 °C / |Inert atmosphere 2: sulfuric acid / 2.5 h / 90 °C / |Inert atmosphere 3: sodium hydroxide; dihydrogen peroxide / water / 0 - 20 °C / |Inert atmosphere 4: hydrogenchloride / water / 12 h / |Reflux; |Inert atmosphere 5: palladium 10 on activated carbon; hydrogen / methanol / 8 h / |Inert atmosphere 6: water / 0.75 h / |Reflux; |Inert atmosphere View Scheme
参考文献
Wang, Jingjing; Zuo, Sujing; Chen, Weiqiang; Zhang, Xinrui; Tan, Kaixin; Tian, Yun; Wang, Jianhui
Journal of Organic Chemistry, 2013 , vol. 78, # 17 p. 8217 - 8231