5-甲酰基-2-甲氧基苯基 乙酸酯合成路线 （共 20 条）
反应条件
1: 87.5 percent / m-chloroperbenzoic acid / CH2Cl2 / 2.5 h / Heating 2: Cs2CO3 / dimethylformamide / 5 h / Ambient temperature View Scheme
参考文献
Aihara, Kazuhiro; Urano, Yasuteru; Higuchi, Tsunehiko; Hirobe, Masaaki
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 11 p. 2165 - 2170
反应条件
1: 87.5 percent / m-chloroperbenzoic acid / CH2Cl2 / 2.5 h / Heating 2: Cs2CO3 / dimethylformamide / 5 h / Ambient temperature 3: 25percent aq. NH3 / dimethylformamide / 0.5 h View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 11 p. 2165 - 2170
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane 2.5 h; Heating;
参考文献
Aihara, Kazuhiro; Urano, Yasuteru; Higuchi, Tsunehiko; Hirobe, Masaaki
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 11 p. 2165 - 2170
反应条件
1: potassium bromide; bromine / water / 20 °C 2: hydrogenchloride / water / 10 h / 90 °C 3: ethanol / 18 h / |Reflux View Scheme
参考文献
Chen, Han; Long, Haitao; Cui, Xiaojie; Zhou, Jiang; Xu, Ming; Yuan, Gu
Journal of the American Chemical Society, 2014 , vol. 136, # 6 p. 2583 - 2591
反应条件
1: 87.5 percent / m-chloroperbenzoic acid / CH2Cl2 / 2.5 h / Heating 2: 99 percent / 25percent aq. NH3 / methanol / 2 h / Ambient temperature View Scheme
参考文献
Aihara, Kazuhiro; Urano, Yasuteru; Higuchi, Tsunehiko; Hirobe, Masaaki
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 11 p. 2165 - 2170
反应条件
1: potassium bromide; bromine / water / 20 °C 2: hydrogenchloride / water / 10 h / 90 °C View Scheme
参考文献
Chen, Han; Long, Haitao; Cui, Xiaojie; Zhou, Jiang; Xu, Ming; Yuan, Gu
Journal of the American Chemical Society, 2014 , vol. 136, # 6 p. 2583 - 2591
反应条件
1: iodine; sodium acetate; acetic acid; bromine
2: glacial acetic acid; sodium acetate; bromine
View Scheme
参考文献
Raiford; Ravely
Journal of Organic Chemistry, 1940 , vol. 5, p. 204,208
反应条件
1.1: CH2Cl2 / Heating
2.1: H2 / 10 percent Pd/C / ethyl acetate / 20 °C
2.2: LiAlH4 / tetrahydrofuran / Heating
View Scheme
参考文献
Fronza, Giovanni; Fuganti, Claudio; Serra, Stefano; Cisero, Marco; Koziet, Joseph
Journal of agricultural and food chemistry, 2002 , vol. 50, # 10 p. 2748 - 2754
反应条件
bromine; iodine; sodium acetate; acetic acid
参考文献
Raiford; Ravely
Journal of Organic Chemistry, 1940 , vol. 5, p. 204,208
参考文献
Raiford; Ravely
Journal of Organic Chemistry, 1940 , vol. 5, p. 204,208
