1,1,1,3,3,3-hexachloro-propan-2-one; triphenylphosphine 3 h; Ambient temperature;

1: 78 percent / lithium aluminum hydride / diethyl ether / Heating 2: 85 percent / hexachloroacetone, triphenylphosphine / 3 h / Ambient temperature View Scheme

silver(I) acetate T=115°C; 48 h;