硫代苯甲酸 S-苯基酯合成路线 （共 180 条）
反应条件
in tetrachloromethane
Kinetics; Me3GeSPh heated with equimolar amt. of PhCOCl in CCl4 in sealed tube at120°C for 30 h; distn.;
参考文献
Kozuka, Seizi; Tamura, Shoji; Yamazaki, Tetsuya; Yamaguchi, Shigeru; Tagaki, Waichiro
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, p. 3277 - 3281
反应条件
in toluene
1.) 16 h, 2.) reflux, 2.5 h;
参考文献
Hanefeld, Wolfgang; Bercin, Erdogan
Archiv der Pharmazie (Weinheim, Germany), 1984 , vol. 317, # 1 p. 74 - 79
反应条件
1: 21 percent / p-TsOH / benzene / Heating
2: 1.) LDA / 1.) THF, -78 deg C, 10 min, 2.) THF, -78 deg C, 15 min
3: 95 percent / m-CPBA / CH2Cl2 / 0.17 h / Ambient temperature
View Scheme
参考文献
Kang, Yoon Ho; Kim, Kyongtae
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 6 p. 1741 - 1752
反应条件
1: 1.) LDA / 1.) THF, -78 deg C, 10 min, 2.) THF, -78 deg C, 15 min
2: 95 percent / m-CPBA / CH2Cl2 / 0.17 h / Ambient temperature
View Scheme
参考文献
Kang, Yoon Ho; Kim, Kyongtae
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 6 p. 1741 - 1752
反应条件
1: 50 percent / PhCOOH, LiClO4, alumina, MeCN, PhSH / acetonitrile / 2 h / constant current electrolysis: 100 mA, graphite cell, platine anode
2: 85 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene / benzene / 24 h / Ambient temperature
View Scheme
参考文献
Ohmori, Hidenobu; Maeda, Hatsuo; Konomoto, Kohichi; Sakai, Kiyoshi; Masui, Masaichiro
Chemical and Pharmaceutical Bulletin, 1987 , vol. 35, # 11 p. 4473 - 4481
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=20 - 25°C; 3 h; Kinetics; TemperatureTime;
参考文献
Os'kina; Vlasov
Russian Journal of Organic Chemistry, 2008 , vol. 44, # 4 p. 561 - 569
反应条件
phenyl-magnesium bromide in tetrahydrofuran; diethyl ether
T=65°C; Tishchenko reaction; 4 h; Inert atmosphere;
参考文献
Cronin, Linda; Manoni, Francesco; O'Connor, Cornelius J.; Connon, Stephen J.
Angewandte Chemie - International Edition, 2010 , vol. 49, # 17 p. 3045 - 3048
反应条件
hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; bis(1,2-diphenylphosphino)benzene in chlorobenzene
6 h; Inert atmosphereReflux;
参考文献
Li, Guangzhe; Arisawa, Mieko; Yamaguchi, Masahiko
Chemical Communications, 2014 , vol. 50, # 33 p. 4328 - 4330
反应条件
aluminum oxide; lithium perchlorate; benzoic acid in acetonitrile
12 h; Ambient temperature;
参考文献
Ohmori, Hidenobu; Maeda, Hatsuo; Konomoto, Kohichi; Sakai, Kiyoshi; Masui, Masaichiro
Chemical and Pharmaceutical Bulletin, 1987 , vol. 35, # 11 p. 4473 - 4481
反应条件
pyridine in various solvent(s)
192 h; Ambient temperature; Yield given;
参考文献
Saegusa, Yasuo; Watanabe, Tatsushi; Nakamura, Shigeo
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 2 p. 539 - 544
