in carbon disulfide byproducts: C6H10S6; air atm.; equimolar ratio, stirring, pptn.; filtn. (SiO2);

in benzene (exclusion of moisture), ligand and Ti complex stirred in benzene at 30-40°C for 180 min; evapd.(vac.), dissolved (CS2), treated with n-pentane, cooled to -26°C for 15 h, isolated, washed (n-pentane), dried (air), elem. anal.;

in carbon disulfide byproducts: C6H10S11; air atm.; equimolar ratio, stirring, pptn.; filtn. (SiO2);