2-(4-甲氧基苄基)-1,3,3-三甲基-4-哌啶酮合成路线 （共 4 条）
反应条件
1: 2: With hydrogen; palladium on activated charcoal Further stages.;
参考文献
Thomas, James B.; Brieaddy, Lawrence E.; Boldt, Karl G.; Perretta, Carin; Carroll, F. Ivy
Synthesis, 2007 , # 10 p. 1481 - 1484
反应条件
in tetrahydrofuran T=20°C;
参考文献
Thomas, James B.; Brieaddy, Lawrence E.; Boldt, Karl G.; Perretta, Carin; Carroll, F. Ivy
Synthesis, 2007 , # 10 p. 1481 - 1484
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
0.5 h; cooling;
参考文献
Thomas, James B.; Brieaddy, Lawrence E.; Boldt, Karl G.; Perretta, Carin; Carroll, F. Ivy
Synthesis, 2007 , # 10 p. 1481 - 1484
反应条件
1.1: 79 percent / sodium hydride / tetrahydrofuran / 0.75 h / cooling
2.1: BuLi; i-Pr2NH / hexane; tetrahydrofuran / 1 h / -78 °C
2.2: 68 percent / hexane; tetrahydrofuran / 2 h / -78 - 20 °C
3.1: 66 percent / lithium aluminum hydride / tetrahydrofuran / 0.5 h / cooling
View Scheme
参考文献
Thomas, James B.; Brieaddy, Lawrence E.; Boldt, Karl G.; Perretta, Carin; Carroll, F. Ivy
Synthesis, 2007 , # 10 p. 1481 - 1484
