1-三氟甲基-1,2-苯碘酰-3(H)-酮合成路线 （共 52 条）
反应条件
caesium carbonate in water; acetonitrile
T=25°C; 24 h; Inert atmosphereSchlenk techniqueSealed tube;
参考文献
Ji, Guojing; Wang, Xi; Zhang, Songnan; Xu, Yan; Ye, Yuxuan; Li, Ming; Zhang, Yan; Wang, Jianbo
Chemical Communications, 2014 , vol. 50, # 33 p. 4361 - 4363
反应条件
N,N,N',N,-tetramethylethylenediamine; copper diacetate in dichloromethane; water
T=20°C; 24 h; Reagent/catalystSolventTemperatureTime;
参考文献
He, Zhengbiao; Zhang, Rui; Hu, Mingyou; Li, Lingchun; Ni, Chuanfa; Hu, Jinbo
Chemical Science, 2013 , vol. 4, # 9 p. 3478 - 3483
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane
T=20°C; 0.0833333 h; Schlenk techniqueInert atmosphere;
参考文献
Miyazaki, Ayako; Shimizu, Ryo; Egami, Hiromichi; Sodeoka, Mikiko
Heterocycles, 2012 , vol. 86, # 2 p. 979 - 983
反应条件
1,10-phenanthroline; tetrabutyl ammonium fluoride; cupric trifluoroacetate in dimethyl sulfoxide
T=130°C; 8 h; Inert atmosphereSealed tube;
参考文献
Lin, Xiaoxi; Wang, Guimei; Li, Huaifeng; Huang, Yuanyuan; He, Weiming; Ye, Dandan; Huang, Kuo-Wei; Yuan, Yaofeng; Weng, Zhiqiang
Tetrahedron, 2013 , vol. 69, # 12 p. 2628 - 2632
反应条件
1,10-phenanthroline; tetrabutyl ammonium fluoride; cupric trifluoroacetate in dimethyl sulfoxide
T=130°C; 8 h; Inert atmosphereSealed tube; SolventReagent/catalystTemperatureTime;
参考文献
Lin, Xiaoxi; Wang, Guimei; Li, Huaifeng; Huang, Yuanyuan; He, Weiming; Ye, Dandan; Huang, Kuo-Wei; Yuan, Yaofeng; Weng, Zhiqiang
Tetrahedron, 2013 , vol. 69, # 12 p. 2628 - 2632
反应条件
[iridium(III)(2-phenylpyridine)3] in N,N-dimethyl-formamide
T=20°C; Inert atmosphereIrradiationSchlenk technique;
参考文献
Xie, Jin; Yuan, Xiangai; Abdukader, Ablimit; Zhu, Chengjian; Ma, Jing
Organic Letters, 2014 , vol. 16, # 6 p. 1768 - 1771
反应条件
18-crown-6 ether in N,N-dimethyl-formamide
T=-60 - 20°C;
参考文献
Stanek, Kyrill; Koller, Raffael; Togni, Antonio
Journal of Organic Chemistry, 2008 , vol. 73, # 19 p. 7678 - 7685
反应条件
caesium carbonate in water; acetonitrile
T=25°C; 24 h; Inert atmosphereSchlenk techniqueSealed tube;
参考文献
Ji, Guojing; Wang, Xi; Zhang, Songnan; Xu, Yan; Ye, Yuxuan; Li, Ming; Zhang, Yan; Wang, Jianbo
Chemical Communications, 2014 , vol. 50, # 33 p. 4361 - 4363
反应条件
1,10-phenanthroline; tetrabutyl ammonium fluoride; cupric trifluoroacetate in dimethyl sulfoxide
T=130°C; 8 h; Inert atmosphereSealed tube;
参考文献
Lin, Xiaoxi; Wang, Guimei; Li, Huaifeng; Huang, Yuanyuan; He, Weiming; Ye, Dandan; Huang, Kuo-Wei; Yuan, Yaofeng; Weng, Zhiqiang
Tetrahedron, 2013 , vol. 69, # 12 p. 2628 - 2632
反应条件
copper (I) cyanide; 4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl-4',4',5',5'-tetramethyl-1,3,2-dioxaborolane in chloroform-d1
T=20°C; 18 h; Reagent/catalystTemperatureConcentrationSolvent;
参考文献
Ilchenko, Nadia O.; Janson, Paer G.; Szabo, Kalman J.
Chemical Communications, 2013 , vol. 49, # 59 p. 6614 - 6616
