3-氯丙基二甲基乙烯基硅烷合成路线 （共 8 条）
反应条件
1: dibenzoyl peroxide; hydrogen bromide / hexane / 6 h / |Inert atmosphere; |UV-irradiation 2: trifluoro-methanesulfonic acid amide; triethylamine / tetrahydrofuran / 13 h / |Inert atmosphere; |Reflux View Scheme
参考文献
Suslova; Albanov; Shainyan
Russian Journal of General Chemistry, 2013 , vol. 83, # 3 p. 453 - 461
Zh. Obshch. Khim., 2013 , vol. 83, # 3 p. 399 - 407,9
反应条件
1: dibenzoyl peroxide; hydrogen bromide / hexane / 6 h / |Inert atmosphere; |UV-irradiation 2: triethylamine / methanol / |Reflux View Scheme
参考文献
Suslova; Albanov; Shainyan
Russian Journal of General Chemistry, 2013 , vol. 83, # 3 p. 453 - 461
Zh. Obshch. Khim., 2013 , vol. 83, # 3 p. 399 - 407,9
反应条件
hydrogenchloride; chlorobis(cyclooctene)rhodium(I) dimer in 1,4-dioxane; chloroform T=20°C; 2 h;
参考文献
Park, Jung-Woo; Jun, Chul-Ho
Organic Letters, 2007 , vol. 9, # 20 p. 4073 - 4076
反应条件
1: in tetrahydrofuran
T=0°C; 2 h;
2: With ammonium chloride in tetrahydrofuran; water
参考文献
INDUSTRY-ACADEMIC COOPERATION FOUNDATION, YONSEI UNIVERSITY
Patent: WO2007/120014 A1, 2007 ;
Location in patent: Page/Page column 33-35 ;
参考文献
Voronkov, M. G.; Kirpichenko, S. V.; Abrosimova, A. T.; Albanov, A. I.; Keiko, V. V.; Lavrent'yev, V. I.
Journal of Organometallic Chemistry, 1987 , vol. 326, p. 159 - 168
反应条件
1:
2: With vinyl-magnesium chloride in tetrahydrofuran
参考文献
Park, Jung-Woo; Park, Sung Joon; Jun, Chul-Ho
Organic Letters, 2012 , vol. 14, # 6 p. 1468 - 1471
反应条件
1: 98 percent / Bu4NI / dimethylformamide / 20 h / 85 - 90 °C
2: 42 percent / NH3 / ethanol / 0.67 h / Ambient temperature
View Scheme
参考文献
Tolstikova; Shainyan
Russian Journal of General Chemistry, 1997 , vol. 67, # 11 p. 1728 - 1732
反应条件
potassium hydrosulphide in ethanol
2 h; Heating;
参考文献
Voronkov, M. G.; Kirpichenko, S. V.; Suslova, E. N.; Keiko, V. V.; Albanov, A. I.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 10 p. 2404 - 2405,2169 - 2170
