4-氯-2-异丙基-5-甲基苯酚合成路线 (共 27 条)
反应条件
oxygen; lithium chloride; copper dichloride in acetic acid T=80°C; P=760.051 Torr; 4 h;
参考文献
Menini, Luciano; Gusevskaya, Elena V.
Chemical Communications, 2006 , # 2 p. 209 - 211
反应条件
1: With triethylamine in N,N-dimethyl-formamide; toluene Curtius rearrangement; 3 h; Heating; 2: With potassium hydroxide; glycerol in ethanol; N,N-dimethyl-formamide; toluene 2 h; Heating; Further stages.;
参考文献
Spurg, Anke; Waldvogel, Siegfried R.
European Journal of Organic Chemistry, 2008 , # 2 p. 337 - 342
反应条件
sulfuric acid; acetic acid
参考文献
Journal of the American Chemical Society, , vol. 54, p. 1063,1069
参考文献
Journal of the American Chemical Society, , vol. 73, p. 2723
反应条件
1,1-dimethyl-4-chloro-3,5-cyclohexanedione; dihydrogen peroxide; sodium chloride in aq. buffer T=25°C; pH=2.75; Electrochemical reactionEnzymatic reaction; ConcentrationTimeTemperaturepH-value;
参考文献
Green Chemistry, , vol. 16, # 3 p. 1104 - 1108
反应条件
sulfuric acid; anhydrous zinc sulfate T=0°C; Diazotization.Behandeln mit Kupfer(I)-chlorid-Loesung;
参考文献
DE431513 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 15, p. 215
反应条件
Fuller's Earth T=140 - 160°C;
反应条件
zinc(II) chloride T=80 - 90°C;
参考文献
DE555904 , ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 18, p. 2949
反应条件
Fuller's Earth T=160 - 185°C;
反应条件
sulfuric acid T=80 - 85°C;
参考文献
DE531774 , ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 17, p. 2543