titanium(IV) isopropylate; (R)-2,2'-dihydroxy-1,1'-binaphthyl in tetrahydrofuran; toluene T=0°C; 5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
1: diethylzinc; phenylacetylene With chiral bicyclo[3.2.1]octane-based alcohol in tetrahydrofuran; hexane 1 h; 2: 2-chloro-benzaldehyde in tetrahydrofuran; hexane T=0°C; 6 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Scarpi, Dina; Galbo, Fabrizio Lo; Guarna, Antonio
Tetrahedron Asymmetry, 2006 , vol. 17, # 9 p. 1409 - 1414
