5-丙二烯基-2-吡咯烷酮合成路线 （共 5 条）
反应条件
boron trifluoride diethyl etherate in acetonitrile
T=-20 - 20°C;
参考文献
Breman, Arjen C.; Dijkink, Jan; Van Maarseveen, Jan H.; Kinderman, Sape S.; Hiemstra, Henk
Journal of Organic Chemistry, 2009 , vol. 74, # 16 p. 6327 - 6330
反应条件
boron trifluoride diethyl etherate in dichloromethane
T=-20 - 20°C; 0.5 h;
参考文献
Karstens, Willem F.J.; Klomp, Dirk; Rutjes, Floris P.J.T.; Hiemstra, Henk
Tetrahedron, 2001 , vol. 57, # 24 p. 5123 - 5130
反应条件
formic acid
72 h; Ambient temperature;
参考文献
Castelhano,A.L.; Krantz,A.
Journal of the American Chemical Society, 1984 , vol. 106, p. 1877
反应条件
1: 65 percent / sodium borohydride / methanol / 0 °C
2: 35 percent / 95-97percent HCO2H / 72 h / Ambient temperature
View Scheme
参考文献
Castelhano,A.L.; Krantz,A.
Journal of the American Chemical Society, 1984 , vol. 106, p. 1877
反应条件
1: 45 percent / Ph3P, diethyl azodicarboxylate / tetrahydrofuran
2: 65 percent / sodium borohydride / methanol / 0 °C
3: 35 percent / 95-97percent HCO2H / 72 h / Ambient temperature
View Scheme
参考文献
Castelhano,A.L.; Krantz,A.
Journal of the American Chemical Society, 1984 , vol. 106, p. 1877
