反应条件
1: hydrogenchloride; sodium nitrite; tin(ll) chloride / water / 0.75 h / 0 - 5 °C / |Inert atmosphere
2: sodium hydroxide / tetrahydrofuran / 0.5 h / |Inert atmosphere
3: [{(η5-C5Me5)RhCl}2(μ-Cl)2]; caesium acetate; acetic acid / 1,2-dichloro-ethane / 16 h / 100 °C / |Inert atmosphere
View Scheme
参考文献
Zhao, Dongbing; Shi, Zhuangzhi; Glorius, Frank
Angewandte Chemie - International Edition, 2013 , vol. 52, # 47 p. 12426 - 12429
Angew. Chem., 2013 , vol. 125, # 47 p. 12652 - 12656,4
