N-(3-噻吩基甲基)环己胺合成路线 （共 2 条）
反应条件
chloro[(tri-tert-butylphosphine)-2-(2-aminobiphenyl)]palladium(II); caesium carbonate in tetrahydrofuran; water
T=75°C; Suzuki-Miyaura cross-coupling reaction; 24 h; Inert atmosphere;
参考文献
Fleury-Bregeot, Nicolas; Raushel, Jessica; Sandrock, Deidre L.; Dreher, Spencer D.; Molander, Gary A.
Chemistry - A European Journal, 2012 , vol. 18, # 31 p. 9564 - 9570
反应条件
1: tetrahydrofuran; tert-butyl alcohol / 12 h / 60 °C
2: chloro[(tri-tert-butylphosphine)-2-(2-aminobiphenyl)]palladium(II); caesium carbonate / tetrahydrofuran; water / 24 h / 75 °C / Inert atmosphere
View Scheme
参考文献
Fleury-Bregeot, Nicolas; Raushel, Jessica; Sandrock, Deidre L.; Dreher, Spencer D.; Molander, Gary A.
Chemistry - A European Journal, 2012 , vol. 18, # 31 p. 9564 - 9570
