3-溴-4-氨基-5-硝基吡啶合成路线 （共 11 条）
反应条件
bromine; sodium acetate; acetic acid T=100°C; Sealed tube; TimeConcentration;
参考文献
Samumed, LLC; Hood, John; Kumar KC, Sunil; Wallace, David Mark
Patent: US2013/296302 A1, 2013 ;
Location in patent: Paragraph 0563 ;
反应条件
potassium thioacyanate; acetic acid
参考文献
Pharmaceutical Bulletin, , vol. 4, p. 20,23
反应条件
sulfuric acid T=175°C; 16 h; Yield given;
参考文献
Polish Journal of Chemistry, , vol. 69, # 4 p. 605 - 611
反应条件
sulfuric acid T=175°C; 16 h; Yield given;
参考文献
Polish Journal of Chemistry, , vol. 69, # 4 p. 605 - 611
反应条件
1.1: sulfuric acid; nitric acid / 5.5 h / 10 - 20 °C 2.1: sulfuric acid / 20 - 90 °C 3.1: potassium acetate; acetic acid / 1 h / 20 °C 3.2: 20 °C View Scheme
参考文献
Synthesis, , # 5 p. 794 - 806
反应条件
1.1: sulfuric acid / 20 - 90 °C 2.1: potassium acetate; acetic acid / 1 h / 20 °C 2.2: 20 °C View Scheme
参考文献
Synthesis, , # 5 p. 794 - 806
参考文献
Pharmaceutical Bulletin, , vol. 4, p. 20,23
参考文献
Chemische Berichte, , vol. 57, p. 1183
反应条件
water; tin(ll) chloride in ethanol 2 h; Reflux;
参考文献
Antoine, Maud; Czech, Michael; Gerlach, Matthias; Guenther, Eckhard; Schuster, Tilmann; Marchand, Pascal
Synthesis, 2011 , # 5 p. 794 - 806
反应条件
hydrogenchloride; tin(ll) chloride in ethanol; water T=20°C; 5 h;
参考文献
Antoine, Maud; Czech, Michael; Gerlach, Matthias; Guenther, Eckhard; Schuster, Tilmann; Marchand, Pascal
Synthesis, 2011 , # 5 p. 794 - 806
