2-n-(乙酰基氨基)-二甲基膦乙酸甲酯合成路线 （共 16 条）
反应条件
hydrogen; palladium on activated charcoal in methanol P=2280 Torr; 3 h;
参考文献
Synthesis, , # 1 p. 53 - 60
反应条件
1: N-acetyl-α-methoxyglycine methyl ester With phosphorus trichoride in toluene T=70°C; 17 h; 2: phosphorous acid trimethyl ester in toluene T=70°C; 2 h;
参考文献
US2007/197429 A1, ;
Page/Page column 56 ;
反应条件
1: With triphenyl-methyl-phosphonium iodide in dichloromethane T=20 - 45°C; Michaelis-Arbuzov rearrangement; 2: With methyl iodide in dichloromethane T=20°C; 24 h;
参考文献
Tetrahedron Letters, , vol. 47, # 20 p. 3439 - 3442
反应条件
in dichloromethane 2 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 12 p. 1603 - 1610
反应条件
dirhodium tetraacetate in toluene T=110°C; 3.5 h;
参考文献
Synthesis, , # 20 art. no. T06405SS, p. 3571 - 3580
反应条件
1: SOCl2 / CH2Cl2 / 1 h / Heating 2: toluene / 80 °C View Scheme
参考文献
Synthetic Communications, , vol. 20, # 22 p. 3395 - 3401
反应条件
in toluene T=80°C; Yield given;
参考文献
Synthetic Communications, , vol. 20, # 22 p. 3395 - 3401
参考文献
Tetrahedron Letters, , vol. 30, # 38 p. 5121 - 5124
参考文献
Tetrahedron Letters, , vol. 30, # 38 p. 5121 - 5124
反应条件
1: 92 percent / DBU 2: 84 percent / NBS, Et3N View Scheme
参考文献
Hoerrner, R. Scott; Askin, David; Volante, R. P.; Reider, Paul J.
Tetrahedron Letters, 1998 , vol. 39, # 21 p. 3455 - 3458
