您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
898909-69-8
合成路线
（共 4 条）
898909-69-8
→
反应条件
868526-38-9
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=45°C; 3 h;
参考文献
Caijo, Frederic; Mosset, Paul; Gree, Rene; Audinot-Bouchez, Valerie; Boutin, Jean; Renard, Pierre; Caignard, Daniel-Henri; Dacquet, Catherine
European Journal of Organic Chemistry, 2006 , # 9 p. 2181 - 2196
868526-35-6
→
反应条件
898909-69-8
反应条件
<b>Multi-step reaction with 2 steps<br /> </b>1.1: 86 percent / imidazole / dimethylformamide / 24 h / 20 °C<br />2.1: n-BuLi / tetrahydrofuran / 0.33 h / -80 °C<br />2.2: 68 percent / HMPA / tetrahydrofuran / 0 °C<br /> <br />
参考文献
Caijo, Frederic; Mosset, Paul; Gree, Rene; Audinot-Bouchez, Valerie; Boutin, Jean; Renard, Pierre; Caignard, Daniel-Henri; Dacquet, Catherine European Journal of Organic Chemistry, 2006 , # 9 p. 2181 - 2196
628-17-1
1-碘戊烷
→
反应条件
898909-69-8
反应条件
<b>Multi-step reaction with 4 steps<br /> </b>1.1: 78 percent / KOH / dimethylsulfoxide / 16 h / 80 °C<br />2.1: Mg; mercury(II) chloride / diethyl ether / 0.5 h / Heating<br />2.2: 78 percent / diethyl ether / 0.33 h / -80 °C<br />3.1: 86 percent / imidazole / dimethylformamide / 24 h / 20 °C<br />4.1: n-BuLi / tetrahydrofuran / 0.33 h / -80 °C<br />4.2: 68 percent / HMPA / tetrahydrofuran / 0 °C<br /> <br />
参考文献
Caijo, Frederic; Mosset, Paul; Gree, Rene; Audinot-Bouchez, Valerie; Boutin, Jean; Renard, Pierre; Caignard, Daniel-Henri; Dacquet, Catherine European Journal of Organic Chemistry, 2006 , # 9 p. 2181 - 2196
89-95-2
2-甲基苯甲醇
→
反应条件
898909-69-8
反应条件
<b>Multi-step reaction with 4 steps<br /> </b>1.1: 78 percent / KOH / dimethylsulfoxide / 16 h / 80 °C<br />2.1: Mg; mercury(II) chloride / diethyl ether / 0.5 h / Heating<br />2.2: 78 percent / diethyl ether / 0.33 h / -80 °C<br />3.1: 86 percent / imidazole / dimethylformamide / 24 h / 20 °C<br />4.1: n-BuLi / tetrahydrofuran / 0.33 h / -80 °C<br />4.2: 68 percent / HMPA / tetrahydrofuran / 0 °C<br /> <br />
参考文献
Caijo, Frederic; Mosset, Paul; Gree, Rene; Audinot-Bouchez, Valerie; Boutin, Jean; Renard, Pierre; Caignard, Daniel-Henri; Dacquet, Catherine European Journal of Organic Chemistry, 2006 , # 9 p. 2181 - 2196
