3-[(叔丁基二甲基甲硅烷基)氧基]-1-丙醇合成路线 （共 37 条）
反应条件
thionyl chloride; dimethyl sulfoxide; triethylamine in dichloromethane T=-78 - 20°C; Swern oxidation;
参考文献
Kim, Youngsoon; Fuchs, Philip L.
Organic Letters, 2007 , vol. 9, # 13 p. 2445 - 2448
反应条件
1: With ozone in dichloromethane T=-78°C; 0.166667 h; 2: With triphenylphosphine on polystyrene in dichloromethane T=20°C; 14 h;
参考文献
Storer, R. Ian; Takemoto, Toshiyasu; Jackson, Philip S.; Brown, Dearg S.; Baxendale, Ian R.; Ley, Steven V.
Chemistry - A European Journal, 2004 , vol. 10, # 10 p. 2529 - 2547
反应条件
4-methylmorpholine N-oxide; silica gel in dichloromethane; acetonitrile
参考文献
Gong, Leyi; Grupe, Andrew; Peltz, Gary Allen
Patent: US2002/52397 A1, 2002 ;
US 20020052397 A1
反应条件
diisobutylaluminium hydride in diethyl ether T=0 - 20°C; 2 h;
参考文献
White; Blakemore; Browder; Hong; Lincoln; Nagornyy; Robarge; Wardrop
Journal of the American Chemical Society, 2001 , vol. 123, # 35 p. 8593 - 8595
反应条件
1: With ozone in dichloromethane T=-78°C; 0.333333 h; 2: With diphenylphosphinopolystyrene in dichloromethane T=-78 - 20°C; 12 h;
参考文献
Storer, R. Ian; Takemoto, Toshiyasu; Jackson, Philip S.; Ley, Steven V.
Angewandte Chemie - International Edition, 2003 , vol. 42, # 22 p. 2521 - 2525
反应条件
diisobutylaluminium hydride in dichloromethane T=-78°C; 1.5 h;
参考文献
Tredwell, Matthew; Luft, Jennifer A. R.; Schuler, Marie; Tenza, Kenny; Houk, Kendall N.; Gouverneur, Veronique
Angewandte Chemie - International Edition, 2008 , vol. 47, # 2 p. 357 - 360
反应条件
water; C46H53F3N4O4P2RuS in acetone T=69 - 72°C; anti-Markovnikov hydration; 36 h;
参考文献
Grotjahn, Douglas B.; Incarvito, Christopher D.; Rheingold, Arnold L.
Angewandte Chemie - International Edition, 2001 , vol. 40, # 20 p. 3884 - 3887
反应条件
1: imidazole; DMAP / dimethylformamide / 0 - 20 °C 2: TEMPO; potassium bromide; sodium hypochlorite / sodium carbonate; sodium bicarbonate / CH2Cl2; H2O / 0.5 h / pH 8.6 View Scheme
参考文献
Organic Letters, , vol. 9, # 19 p. 3857 - 3858
反应条件
triethylamine in dichloromethane; dimethyl sulfoxide
反应条件
anhydrous potassium hydrogen sulfate; dimethyl sulfoxide; triethylamine in dichloromethane; water
