SCl2; triethylamine in diethyl ether
-78 degC then allowed to warm to room temperature then reflux for 30 min;
参考文献
Daley, Stephen T. A. K.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 207 - 210
aluminium trichloride; tetrasulphure tetranitride in toluene
13 h; Heating;
参考文献
Daley, Stephen T. A. K.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 207 - 210
tetrasulphure tetranitride in toluene
48 h; Heating;
参考文献
Daley, Stephen T. A. K.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 207 - 210
1: diethyl ether / Ambient temperature
2: 65 percent / 70 percent HClO4, acetic anhydride / 2 h / 60 °C
3: 50 percent / NaN3 / acetonitrile / 24 h / Ambient temperature
View Scheme
参考文献
Yonemoto, Katsumi; Shibuya, Isao; Tsuchiya, Tohru; Masahiko Yasumoto; Taguchi, Yoichi
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 10 p. 2933 - 2937
1: NH2OSO3H, NaOH / H2O; diethyl ether / 0.25 h / ice-cooling
2: diethyl ether / Ambient temperature
3: 65 percent / 70 percent HClO4, acetic anhydride / 2 h / 60 °C
4: 50 percent / NaN3 / acetonitrile / 24 h / Ambient temperature
View Scheme
参考文献
Yonemoto, Katsumi; Shibuya, Isao; Tsuchiya, Tohru; Masahiko Yasumoto; Taguchi, Yoichi
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 10 p. 2933 - 2937
1: 65 percent / 70 percent HClO4, acetic anhydride / 2 h / 60 °C
2: 50 percent / NaN3 / acetonitrile / 24 h / Ambient temperature
View Scheme
参考文献
Yonemoto, Katsumi; Shibuya, Isao; Tsuchiya, Tohru; Masahiko Yasumoto; Taguchi, Yoichi
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 10 p. 2933 - 2937
1: NaSH / ethanol / 10 h / Heating
2: NH2OSO3H, NaOH / H2O; diethyl ether / 0.25 h / ice-cooling
3: diethyl ether / Ambient temperature
4: 65 percent / 70 percent HClO4, acetic anhydride / 2 h / 60 °C
5: 50 percent / NaN3 / acetonitrile / 24 h / Ambient temperature
View Scheme
参考文献
Yonemoto, Katsumi; Shibuya, Isao; Tsuchiya, Tohru; Masahiko Yasumoto; Taguchi, Yoichi
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 10 p. 2933 - 2937
