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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1-碘萘
合成路线
（共 431 条）
90-14-2
1-碘萘
→
反应条件
24781-50-8
1-萘丙胺
反应条件
1.1: 9-borabicyclo[3.3.1]nonane / tetrahydrofuran / 2 h / 20 °C 1.2: NaOH / Cl2Pd(PPh3)2 / tetrahydrofuran / 1.5 h / 20 °C 2.1: CF3COOH / CH2Cl2 / 1 h / 20 °C View Scheme
参考文献
Nomura, Takashi; Iwaki, Tsutomu; Yasukata, Tatsuro; Nishi, Koichi; Narukawa, Yukitoshi; Uotani, Koichi; Hori, Toshihiko; Miwa, Hideaki
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 24 p. 6615 - 6628
90-14-2
1-碘萘
+
501-65-5
二苯基乙炔
→
反应条件
13638-84-1
反应条件
thallous acetate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=120°C; 36 h;
参考文献
Grigg; Kennewell; Teasdale; Sridharan
Tetrahedron Letters, 1993 , vol. 34, # 1 p. 153 - 156
90-14-2
1-碘萘
+
98-86-2
苯乙酮
→
反应条件
16216-08-3
反应条件
potassium tert-butylate in dimethyl sulfoxide T=70°C; 0.166667 h; Microwave irradiationInert atmosphere;
参考文献
Soria-Castro, Silvia M.; Caminos, Daniel A.; Penenory, Alicia B.
RSC Advances, 2014 , vol. 4, # 34 p. 17490 - 17497
90-14-2
1-碘萘
→
反应条件
14476-01-8
反应条件
1.1: n-BuLi / diethyl ether; hexane / 1 h / -78 °C 1.2: 67 percent / diethyl ether / 12 h / -78 - 20 °C 2.1: 85 percent / CsOH*H2O; 1,4-bis(diphenylphosphino)butane; water / [allylPdCl]2 / dioxane; toluene / 24 h / 110 °C View Scheme
参考文献
Denmark, Scott E.; Ober, Michael H.
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1703 - 1714
90-14-2
1-碘萘
+
2727-71-1
+
78-94-4
→
反应条件
218-16-6
反应条件
norborn-2-ene; palladium diacetate; potassium carbonate; triphenylphosphine in N,N-dimethyl-formamide T=105°C; 24 h; Inert atmosphere; chemoselective reaction;
参考文献
Della Ca, Nicola; Motti, Elena; Mega, Antonio; Catellani, Marta
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 9 p. 1451 - 1454
292638-84-7
+
90-14-2
1-碘萘
→
反应条件
28358-65-8
+
2840-87-1
反应条件
1,3-bis-(diphenylphosphino)propane; triethylamine; palladium diacetate in N,N-dimethyl-formamide T=80°C; 24 h;
参考文献
Cabri, Walter; Candiani, Ilaria; Bedeschi, Angelo; Santi, Roberto
Journal of Organic Chemistry, 1992 , vol. 57, # 13 p. 3558 - 3563
90-14-2
1-碘萘
+
155857-33-3
→
反应条件
28358-65-8
反应条件
bis(η3-allyl-μ-chloropalladium(II)); tetrabutyl ammonium fluoride in tetrahydrofuran T=60°C; 21 h;
参考文献
Hatanaka, Yasuo; Goda, Ken-ichi; Hiyama, Tamejiro
Journal of Organometallic Chemistry, 1994 , vol. 465, # 1-2 p. 97 - 100
90-14-2
1-碘萘
+
818377-74-1
+
818377-76-3
→
反应条件
64770-16-7
反应条件
tetrabutyl ammonium fluoride; copper(l) chloride; bis(η3-allyl-μ-chloropalladium(II)) in N,N-dimethyl-formamide T=45°C; 40 h;
参考文献
Ghosh, Sunil K.; Singh, Rekha; Singh, Gobind C.
European Journal of Organic Chemistry, 2004 , # 20 p. 4141 - 4147
201230-82-2
+
90-14-2
1-碘萘
→
反应条件
64985-86-0
反应条件
1,3-bis-(diphenylphosphino)propane; water; palladium diacetate; triethylamine in N,N-dimethyl-formamide T=20 - 115°C; P=760.051 Torr; 6 h; Inert atmosphereAutoclave;
参考文献
Li, Yang; Xue, Dong; Wang, Chao; Liu, Zhao-Tie; Xiao, Jianliang
Chemical Communications, 2012 , vol. 48, # 9 p. 1320 - 1322
90-14-2
1-碘萘
→
反应条件
65059-24-7
反应条件
1: dimethyl(phenyl)(3-phenylprop-1-en-2-yl)silane With BF3*AcOH in dichloromethane T=0 - 20°C; Inert atmosphere; 2: monoiodonaphthalene With bis(η3-allyl-μ-chloropalladium(II)); tetrabutyl ammonium fluoride in tetrahydrofuran Hiyama cross-coupling; HeatingInert atmosphere;
参考文献
Yonehara, Mitsuhiro; Nakamura, Shinji; Muranaka, Atsuya; Uchiyama, Masanobu
Chemistry - An Asian Journal, 2010 , vol. 5, # 3 p. 452 - 455
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